Browsing by Author "Crain, Sheila"
Now showing items 1-3 of 3
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Isolation, structure elucidation, relative lc-ms response, and in vitro toxicity of azaspiracids from the dinoflagellateazadinium spinosum
Kilcoyne, Jane; Nulty, Ciara; Jauffrais, Thierry; McCarron, Pearse; Herve, Fabienne; Foley, Barry; Rise, Frode; Crain, Sheila; Wilkins, Alistair L.; Twiner, Michael J.; Hess, Philipp; Miles, Christopher O. (American Chemical Society (ACS), 2014-11-26)We identified three new azaspiracids (AZAs) with molecular weights of 715, 815, and 829 (AZA33 (3), AZA34 (4), and AZA35, respectively) in mussels, seawater, and Azadinium spinosum culture. Approximately 700 mu g of 3 and ... -
Structure elucidation, relative lc–ms response and in vitro toxicity of azaspiracids7–10isolated from mussels (mytilus edulis)
Kilcoyne, Jane; Twiner, Michael J.; McCarron, Pearse; Crain, Sheila; Giddings, Sabrina D.; Foley, Barry; Rise, Frode; Hess, Philipp; Wilkins, Alistair L.; Miles, Christopher O. (American Chemical Society (ACS), 2015-05-27)Azaspiracids (AZAs) are marine biotoxins produced by dinoflagellates that can accumulate in shellfish, which if consumed can lead to poisoning events. AZA7-10, 7-10, were isolated from shellfish and their structures, ... -
The preparation of certified calibration solutions for azaspiracid-1, -2, and -3, potent marine biotoxins found in shellfish
Perez, Ruth A.; Rehmann, Nils; Crain, Sheila; LeBlanc, Patricia; Craft, Cheryl; MacKinnon, Shawna; Reeves, Kelley; Burton, Ian W.; Walter, John A.; Hess, Philipp; Quilliam, Michael A.; Melanson, Jeremy E. (Springer Nature, 2010-09-09)The production and certification of a series of azaspiracid (AZA) calibration solution reference materials is described. Azaspiracids were isolated from contaminated mussels, purified by preparative liquid chromatography ...