Browsing by Author "Quilliam, Michael A."
Now showing items 1-3 of 3
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A mussel tissue certified reference material for multiple phycotoxins. part 1: design and preparation
McCarron, Pearse; Emteborg, Håkan; Nulty, Cíara; Rundberget, Thomas; Loader, Jared I.; Teipel, Katharina; Miles, Christopher O.; Quilliam, Michael A.; Hess, Philipp (Springer Nature, 2011-03-17)The development of multi-analyte methods for lipophilic shellfish toxins based on liquid chromatography-mass spectrometry permits rapid screening and analysis of samples for a wide variety of toxins in a single run. Validated ... -
Improved isolation procedure for azaspiracids from shellfish, structural elucidation of azaspiracid-6, and stability studies
Kilcoyne, Jane; Keogh, Adela; Clancy, Ger; LeBlanc, Patricia; Burton, Ian; Quilliam, Michael A.; Hess, Philipp; Miles, Christopher O. (American Chemical Society (ACS), 2012-03-14)Azaspiracids are a group of lipophilic polyether toxins produced by the small dinoflagellate Azadinium spinosum. They may accumulate in shellfish and can result in illnesses when consumed by humans. Research into analytical ... -
The preparation of certified calibration solutions for azaspiracid-1, -2, and -3, potent marine biotoxins found in shellfish
Perez, Ruth A.; Rehmann, Nils; Crain, Sheila; LeBlanc, Patricia; Craft, Cheryl; MacKinnon, Shawna; Reeves, Kelley; Burton, Ian W.; Walter, John A.; Hess, Philipp; Quilliam, Michael A.; Melanson, Jeremy E. (Springer Nature, 2010-09-09)The production and certification of a series of azaspiracid (AZA) calibration solution reference materials is described. Azaspiracids were isolated from contaminated mussels, purified by preparative liquid chromatography ...